Instrument description

guide hall n° 1, thermal guide H24
 
monochromator
CaF2(422)
temperature range -196 < TM/°C < 250
energy range -125 < ΔE/µeV < 150
angular range 81° < θM < 89°
incident energy (TM≥25°C) 16.45 meV
incident wavelength (TM≥25°C) 2.23 Å
energy resolution 8 µeV
deflector
pyrolytic graphite with variable curvature
sample
sample size 3.5 x 3.5 cm2
flux at sample 2 x 104 n cm-2 s-1
analyser
CaF2(422)
Q-range 0.2 < Q-1 < 4.9
Q-resolution ΔQ-1 < 0.1
detectors
monitors2
35 3He detectors1 <Q/Å-1 < 4.9
3He PSD detector0.2 <Q/Å-1 < 0.8
background per detector 0.5 - 4 cpm
sample environment
furnace 300 < T/K < 1900
cryofurnace

2 < T/K < 500

displex5 < T/K < 550

The high energy resolution of the order of a few μeV together with the availability of high momentum transfer (Q<4.9 Å-1) makes the spectrometer IN13 particularly useful for the microscopic study of single particle motions (jump reorientation, rotational and translational diffusion, tunnelling) observed by incoherent neutron scattering. The instrument partly fills the gap of (Q, ω)  space between IN10 and IN5.

Temperature gradient monochromator

The monochromator and analyser CaF2(422) crystals are oriented in near backscattering geometry thereby achieving an energy resolution of a few μeV. The energy of the incident neutrons is scanned by variation of the temperature of the monochromator at a fixed Bragg-angle. In an optional mode the 10 mm thick monochromator crystals are kept at a fixed temperature gradient and energy variation is performed by scanning the monochromator Bragg-angle. This achieves an increased flux at the sample position and slightly increases the energy resolution width.

A vertically curved Graphite deflector focusses the beam onto the sample. The scattered neutrons are energy analysed by a set of seven spherically curved composite crystal analysers, each covering a large solid angle of 0.18 sr. An additional three circular analysers centred around the transmitted beam cover the small-angle region.

The neutron time-of-flight is used to suppress (i) the background of neutrons scattered directly from the sample into the detectors and (ii) second order contamination.

The neutrons are counted with a cylindrical multidetector consisting of 35 3He detector tubes, arranged in staggered circular rows. The small Q range from 0.2 to 0.8 Å-1 is covered by a 3He Position Sensitive Detector (PSD) arranged to see the circular analysers in exact backscattering.